Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A
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To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur. For example, many low-carbon and stabilized stainless steels e. Because it can be run quickly for screening, we often run this test first.
Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Intergranular corrosion shows up as the dark black lines around the grain boundaries. Please refer to the specification for more details. The etch structure praxtice used to classify the specimens are: All five methods within this specification involve exposing specimens to a chemical mixture designed to pfactice corrosive behavior.
If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.
Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.
Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Practice B, also known as the Streicher test, uses weight loss analysis to provide a quantitative measure of the materials performance.
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application.
We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials praactice corrosive environments.
A different ASTM A test ;ractice must be used to quantify the level of corrosion or to disqualify practcie material for use. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
Discover perspectives, resources, and advice from our world-leading Engaged Experts. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.
A recent publication on intergranular corrosion. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. For example, in highly oxidizing solutions, intergranular attack can occur pracice to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions.
Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. Contact us now for pricing or a quote!
The inch-pound equivalents are in parentheses and may be approximate. The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. The Oxalic Acid test is also 2a62 applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.
ASTM A Testing: An Overview of Intergranular Corrosion | Element
These tests do not provide a basis for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking.
These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. Like what you saw? Please specify the maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack.
Work Item s – proposed revisions of this standard. Link to Active This link will always route to the current Active version of the standard. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away.
The Oxalic Acid test is only used to ensure that practcie corrosion exists; samples are labeled either “Acceptable” or “Suspect”.
ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes.
If you are not sure, please contact us for assistance. See Appendix X1 for information regarding test selection.